2024 |
Liu S, Duan L, Shi F, Filippelli GM, Naidu R, 'Concentrations of per- and polyfluoroalkyl substances in vegetables from Sydney and Newcastle, Australia.', J Sci Food Agric, (2024)
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2023 |
Al Amin M, Luo Y, Shi F, Yu L, Liu Y, Nolan A, et al., 'A modified TOP assay to detect per- and polyfluoroalkyl substances in aqueous film-forming foams (AFFF) and soil.', Front Chem, 11 1141182 (2023) [C1]
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Nova |
2021 |
Satake M, Irie R, Holland PT, Harwood DT, Shi F, Itoh Y, et al., 'Brevisulcenals-A1 and A2, Sulfate Esters of Brevisulcenals, Isolated from the Red Tide Dinoflagellate Karenia brevisulcata', Toxins, 13 (2021) [C1]
Two different types of polycyclic ether toxins, namely brevisulcenals (KBTs) and brevisulcatic acids (BSXs), produced by the red tide dinoflagellate Karenia brevisulcata, were the... [more]
Two different types of polycyclic ether toxins, namely brevisulcenals (KBTs) and brevisulcatic acids (BSXs), produced by the red tide dinoflagellate Karenia brevisulcata, were the cause of a toxic incident that occurred in New Zealand in 1998. Four major components, KBT-F,-G,-H, and-I, shown to be cytotoxic and lethal in mice, were isolated from cultured K. brevisulcata cells, and their structures were elucidated by spectroscopic analyses. New analogues, brevisulcenal-A1 (KBT-A1) and brevisulcenal-A2 (KBT-A2), toxins of higher polarity than that of known KBTs, were isolated from neutral lipophilic extracts of bulk dinoflagellate culture extracts. The structures of KBT-A1 and KBT-A2 were elucidated as sulfated analogues of KBT-F and KBT-G, respectively, by NMR and matrix-assisted laser desorption/ionization tandem mass spectrometry (MALDI TOF/TOF), and by comparison with the spectra of KBT-F and KBT-G. The cytotoxicities of the sulfate analogues were lower than those of KBT-F and KBT-G.
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2021 |
Liu W, Su Y, Liu J, Zhang K, Wang X, Chen Y, et al., 'Determination of cyflufenamid residues in 12 foodstuffs by QuEChERS-HPLC-MS/MS', Food Chemistry, 362 (2021) [C1]
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Nova |
2021 |
Wu X, Cai Y, Shi F, Duan L, Zhang Q, Xu N, 'Characterization of allelopathic compounds from the harmful dinoflagellate, Cochlodinium geminatum', Harmful Algae, 107 (2021) [C1]
In 2006, species of Cochlodinium geminatum were first recorded as new, harmful algal bloom (HAB)-forming dinoflagellate, in the Pearl River Estuary, China. Previous studies indica... [more]
In 2006, species of Cochlodinium geminatum were first recorded as new, harmful algal bloom (HAB)-forming dinoflagellate, in the Pearl River Estuary, China. Previous studies indicated that allelopathy (the release of chemical compounds) is an important competitive strategy for C. geminatum in inhibiting the growth of phytoplankton competitors, however, little is known about the allelochemicals produced by this species. In this study, allelopathic compounds were characterized using a series of chromatographic techniques. Methanol extracts from cultures showed significant inhibitory effects towards the co-occurring phytoplankton, Akashiwo sanguinea, and potent hemolytic activity against rabbit erythrocytes. Solid phase extraction (SPE) fractions from a reverse phase SPE column, exhibited inhibitory and synergistic effects on A. sanguinea growth, of which fractions eluted in 80% and 100% methanol showed the strongest allelopathic activity. These fractions were further purified using reverse phase high performance liquid chromatography (HPLC), and six fractions were collected. Three fractions displayed strong inhibitory effects towards A. sanguinea, with 14%¿25% inhibitory rates, but a higher 35% inhibitory rate was observed when fractions were combined, suggesting allelochemicals had synergistic allelopathic effects. Allelopathic activity also exhibited time dependent reduction when stored at -20°C. Furthermore, trypsin digestion and dialysis assays indicated C. geminatum produced multiple allelopathic compounds. Our study demonstrated that species of C. geminatum produced and released multiple allelopathic compounds of low polarity and sufficient hydrophilicity, which elicit important competitive advantages by inhibiting co-occurring phytoplankton, and promoting population growth.
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Nova |
2018 |
Satake M, Irie R, Hamamoto Y, Tachibana K, Holland PT, Harwood DT, et al., 'BREVISULCENAL-G, -H, and -I, POLYCYCLIC ETHER MARINE TOXINS FROM THE DINOFLAGELLATE KARENIA BREVISULCATA', HETEROCYCLES, 96 2096-2105 (2018)
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2018 |
Dorantes-Aranda JJ, Tan JYC, Hallegraeff GM, Campbell K, Ugalde SC, Harwood DT, et al., 'Detection of Paralytic Shellfish Toxins in Mussels and Oysters Using the Qualitative Neogen Lateral-Flow Immunoassay: An Interlaboratory Study', JOURNAL OF AOAC INTERNATIONAL, 101 468-479 (2018)
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2016 |
Irie R, Suzuki R, Tachibana K, Holland PT, Harwood DT, Shi F, et al., 'BREVISULCATIC ACIDS FROM A MARINE MICROALGAL SPECIES IMPLICATED IN A TOXIC EVENT IN NEW ZEALAND', HETEROCYCLES, 92 45-54 (2016)
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2014 |
Harwood DT, Shi F, Satake M, Holland PT, 'A sensitive LC-MS/MS assay for brevisulcenal and brevisulcatic acid toxins produced by the dinoflagellate Karenia brevisulcata', TOXICON, 84 19-27 (2014)
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2014 |
Suzuki R, Irie R, Harntaweesup Y, Tachibana K, Holland PT, Harwood DT, et al., 'Brevisulcatic Acids, Marine Ladder-Frame Polyethers from the Red Tide Dinoflagellate Karenia brevisulcata in New Zealand', ORGANIC LETTERS, 16 5850-5853 (2014)
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2013 |
Selwood AI, Wilkins AL, Munday R, Shi F, Rhodes LL, Holland PT, 'Portimine: a bioactive metabolite from the benthic dinoflagellate Vulcanodinium rugosum', TETRAHEDRON LETTERS, 54 4705-4707 (2013)
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2012 |
Hamamoto Y, Tachibana K, Holland PT, Shi F, Beuzenberg V, Itoh Y, Satake M, 'Brevisulcenal-F: A Polycyclic Ether Toxin Associated with Massive Fish-kills in New Zealand', JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 134 4963-4968 (2012)
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2012 |
Shi F, McNabb P, Rhodes L, Holland P, Webb S, Adamson J, et al., 'The toxic effects of three dinoflagellate species from the genus Karenia on invertebrate larvae and finfish', NEW ZEALAND JOURNAL OF MARINE AND FRESHWATER RESEARCH, 46 149-165 (2012)
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2012 |
Beuzenberg V, Mountfort D, Holland P, Shi F, MacKenzie L, 'Optimization of growth and production of toxins by three dinoflagellates in photobioreactor cultures', JOURNAL OF APPLIED PHYCOLOGY, 24 1023-1033 (2012)
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2012 |
Holland PT, Shi F, Satake M, Hamamoto Y, Ito E, Beuzenberg V, et al., 'Novel toxins produced by the dinoflagellate Karenia brevisulcata', HARMFUL ALGAE, 13 47-57 (2012)
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